5Y92
Crystal structure of ANXUR2 extracellular domain from Arabidopsis thaliana
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRF BEAMLINE BL19U1 |
| Synchrotron site | SSRF |
| Beamline | BL19U1 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2016-04-27 |
| Detector | DECTRIS PILATUS3 6M |
| Wavelength(s) | 0.97791 |
| Spacegroup name | I 4 |
| Unit cell lengths | 103.189, 103.189, 121.738 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 43.151 - 2.004 |
| R-factor | 0.1847 |
| Rwork | 0.184 |
| R-free | 0.20800 |
| Structure solution method | SAD |
| RMSD bond length | 0.009 |
| RMSD bond angle | 1.087 |
| Data scaling software | SCALEPACK |
| Phasing software | SOLVE |
| Refinement software | PHENIX ((1.10.1_2155: ???)) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 50.000 |
| High resolution limit [Å] | 2.000 |
| Number of reflections | 42707 |
| <I/σ(I)> | 34.7 |
| Completeness [%] | 100.0 |
| Redundancy | 13.3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.2M li2SO4 ,0.1M NaAc (pH=4.5), 50% PEG400 |
