5Y7Q
Crystal structure of paFAN1 bound to 2nt 5'flap DNA with gap
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PAL/PLS BEAMLINE 5C (4A) |
Synchrotron site | PAL/PLS |
Beamline | 5C (4A) |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2015-10-05 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.9795 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 80.845, 104.560, 105.243 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 33.710 - 2.700 |
R-factor | 0.1959 |
Rwork | 0.193 |
R-free | 0.24310 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4r8a |
RMSD bond length | 0.009 |
RMSD bond angle | 1.079 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX |
Refinement software | PHENIX ((1.10.1-2155_1069: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | |
High resolution limit [Å] | 2.490 | |
Rmerge | 0.092 | 2.416 |
Rpim | 0.649 | |
Number of reflections | 31458 | |
<I/σ(I)> | 35.5 | |
Completeness [%] | 99.0 | |
Redundancy | 14.4 | |
CC(1/2) | 0.633 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.2 | 291 | 0.1M HEPES (pH7.2), 25%(w/v) PEG 8000, 30mM Gly-gly-gly |