5Y78
Crystal structure of the triose-phosphate/phosphate translocator in complex with inorganic phosphate
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL32XU |
Synchrotron site | SPring-8 |
Beamline | BL32XU |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2015-12-16 |
Detector | RAYONIX MX225HE |
Wavelength(s) | 1.0000 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 106.550, 164.970, 41.420 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 48.866 - 2.100 |
R-factor | 0.1963 |
Rwork | 0.195 |
R-free | 0.22560 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5i20 |
RMSD bond length | 0.002 |
RMSD bond angle | 0.505 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX ((1.10_2155: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.180 |
High resolution limit [Å] | 2.100 | 2.100 |
Number of reflections | 43639 | |
<I/σ(I)> | 11.3 | 1.1 |
Completeness [%] | 99.8 | 100 |
Redundancy | 90.3 | 87 |
CC(1/2) | 0.995 | 0.653 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | LIPIDIC CUBIC PHASE | 6 | 293 | PEG200, MES, (NH4)2HPO4 |
1 | LIPIDIC CUBIC PHASE | 6 | 293 | PEG200, MES, (NH4)2HPO4 |