5Y6H
Crystal structure of YcgR-N domain of YcgR from Escherichia coli
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2016-01-25 |
Detector | RIGAKU SATURN 944 |
Wavelength(s) | 1.5418 |
Spacegroup name | H 3 |
Unit cell lengths | 91.960, 91.960, 32.530 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 16.982 - 1.774 |
R-factor | 0.1736 |
Rwork | 0.171 |
R-free | 0.19320 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5y6f |
RMSD bond length | 0.004 |
RMSD bond angle | 0.770 |
Data reduction software | iMOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX ((1.11.1_2575: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.110 | 1.870 |
High resolution limit [Å] | 1.770 | 1.770 |
Rmerge | 0.054 | 0.319 |
Rpim | 0.017 | 0.100 |
Number of reflections | 9774 | 1396 |
<I/σ(I)> | 26.6 | 7 |
Completeness [%] | 98.5 | 97.6 |
Redundancy | 11 | 10.7 |
CC(1/2) | 0.999 | 0.962 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.6 | 293 | 0.1M MES pH 5.6, 0.01M Magnesium chloride hexahydrate, 1.8M Lithium sulfate |