5Y5Q
Crystal structure of the WSSV dUTPase D88N/R158E mutant in complex with dUTP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U1 |
Synchrotron site | SSRF |
Beamline | BL17U1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2015-12-29 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.9794 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 59.574, 75.527, 113.321 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 22.840 - 1.560 |
R-factor | 0.174 |
Rwork | 0.173 |
R-free | 0.19200 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5y5p |
RMSD bond length | 0.010 |
RMSD bond angle | 1.050 |
Data reduction software | autoPROC (1.0.4) |
Data scaling software | autoPROC (1.0.4) |
Phasing software | PHASER |
Refinement software | BUSTER (2.10.2) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 113.321 | 1.574 |
High resolution limit [Å] | 1.560 | 1.560 |
Rmerge | 0.060 | 1.133 |
Rpim | 0.016 | 0.315 |
Number of reflections | 71914 | 1449 |
<I/σ(I)> | 26.8 | |
Completeness [%] | 97.9 | 78.3 |
Redundancy | 14.5 | 13.6 |
CC(1/2) | 0.999 | 0.714 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 25% (w/v) PEG 1500 |