5Y4U
Crystal structure of Grx domain of Grx3 from Saccharomyces cerevisiae
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U1 |
Synchrotron site | SSRF |
Beamline | BL17U1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2016-03-10 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 1.5418 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 41.195, 45.749, 45.843 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 25.460 - 1.700 |
R-factor | 0.18234 |
Rwork | 0.180 |
R-free | 0.22948 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3zyw |
RMSD bond length | 0.019 |
RMSD bond angle | 1.844 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | MOLREP |
Refinement software | REFMAC (5.7.0032) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 1.700 |
Number of reflections | 10493 |
<I/σ(I)> | 20.7 |
Completeness [%] | 97.0 |
Redundancy | 4.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8 | 289 | 0.1 M Tris-HCl, pH 8.0, 2 M Ammonium sulfate |