5Y3X
Crystal structure of endo-1,4-beta-xylanase from Caldicellulosiruptor owensensis
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL19U1 |
Synchrotron site | SSRF |
Beamline | BL19U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-10-02 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 0.97852 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 126.650, 74.071, 137.744 |
Unit cell angles | 90.00, 90.44, 90.00 |
Refinement procedure
Resolution | 29.113 - 2.100 |
R-factor | 0.1916 |
Rwork | 0.190 |
R-free | 0.22890 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4pmd |
Phasing software | PHASER |
Refinement software | PHENIX (1.11_2567) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 29.113 | 2.180 |
High resolution limit [Å] | 2.100 | 2.100 |
Rmerge | 0.491 | |
Number of reflections | 148527 | |
<I/σ(I)> | 15.3 | 2.5 |
Completeness [%] | 99.9 | 99.6 |
Redundancy | 6.5 | 5.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 294 | 5% Iso-Propanol, 2.2 M (NH4)2SO4 |