5Y1A
HBP35 of Porphyromonas gingivalis
Experimental procedure
| Experimental method | MAD |
| Source type | SYNCHROTRON |
| Source details | PHOTON FACTORY BEAMLINE AR-NW12A |
| Synchrotron site | Photon Factory |
| Beamline | AR-NW12A |
| Temperature [K] | 95 |
| Detector technology | CCD |
| Collection date | 2005-10-22 |
| Detector | ADSC QUANTUM 210 |
| Wavelength(s) | 0.9791 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 49.016, 58.324, 114.417 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 31.930 - 1.800 |
| R-factor | 0.1777 |
| Rwork | 0.176 |
| R-free | 0.21134 |
| RMSD bond length | 0.013 |
| RMSD bond angle | 1.328 |
| Data reduction software | MOLREP |
| Data scaling software | SCALEPACK |
| Phasing software | SOLVE |
| Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | |
| High resolution limit [Å] | 1.800 | |
| Rmerge | 0.081 | 0.395 |
| Number of reflections | 30871 | |
| <I/σ(I)> | 24 | |
| Completeness [%] | 99.5 | |
| Redundancy | 6.5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | BATCH MODE | 293 | 10-15% PEG 400, 20% Ethanol |
