5Y18
Crystal structure of DAXX helical bundle domain in complex with ATRX
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL19U1 |
Synchrotron site | SSRF |
Beamline | BL19U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-01-27 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 0.9785 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 69.485, 107.904, 30.887 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 26.976 - 2.202 |
R-factor | 0.188 |
Rwork | 0.186 |
R-free | 0.21920 |
Structure solution method | SAD |
RMSD bond length | 0.002 |
RMSD bond angle | 0.530 |
Data reduction software | HKL-3000 |
Data scaling software | HKL-3000 |
Phasing software | SHARP |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 2.280 |
High resolution limit [Å] | 2.200 | 4.740 | 2.200 |
Rmerge | 0.077 | 0.053 | 0.413 |
Rmeas | 0.084 | 0.058 | 0.457 |
Rpim | 0.033 | 0.024 | 0.192 |
Total number of observations | 38355 | ||
Number of reflections | 6179 | 677 | 594 |
<I/σ(I)> | 6.6 | ||
Completeness [%] | 99.6 | 98.8 | 99.8 |
Redundancy | 6.2 | 5.8 | 5.4 |
CC(1/2) | 0.995 | 0.901 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | 289 | 0.1M sodium citrate, pH6.5, 0.2M ammonium acetate, 30% PEG4000 |