5Y0Y
RVFV GN-AU
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U1 |
Synchrotron site | SSRF |
Beamline | BL17U1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2016-12-01 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 1.03906 |
Spacegroup name | P 65 2 2 |
Unit cell lengths | 97.180, 97.180, 184.128 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 42.972 - 3.398 |
R-factor | 0.2776 |
Rwork | 0.275 |
R-free | 0.31660 |
Structure solution method | SAD |
RMSD bond length | 0.003 |
RMSD bond angle | 0.653 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX |
Refinement software | PHENIX ((1.11.1_2575: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 3.520 |
High resolution limit [Å] | 3.400 | 3.400 |
Rmerge | 0.887 | |
Number of reflections | 7634 | 740 |
<I/σ(I)> | 23.5 | |
Completeness [%] | 99.9 | 100 |
Redundancy | 14.8 | 15.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 277 | 0.2M ammonium sulfate, 0.1M MES, pH 6.5, 20% (w/v) PEG 8000 |