5Y0R
Crystal structure of Thermotoga maritima TmcAL (apo, form I)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE BL-17A |
Synchrotron site | Photon Factory |
Beamline | BL-17A |
Temperature [K] | 95 |
Detector technology | PIXEL |
Collection date | 2014-12-02 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 0.97884 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 77.448, 77.448, 183.076 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 47.933 - 3.110 |
R-factor | 0.2178 |
Rwork | 0.215 |
R-free | 0.27390 |
Structure solution method | SAD |
RMSD bond length | 0.002 |
RMSD bond angle | 0.595 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX (1.8.4_1496) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 3.190 | |
High resolution limit [Å] | 3.110 | 13.910 | 3.110 |
Rmerge | 0.177 | 0.041 | 1.874 |
Rmeas | 0.183 | 0.043 | 1.948 |
Number of reflections | 19083 | 212 | 1379 |
<I/σ(I)> | 14.14 | 48.35 | 1.72 |
Completeness [%] | 99.9 | 98.1 | 98.6 |
Redundancy | 25 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | Tris, isopropanol, MgCl2 |