5Y0E
Crystal structure of TssK
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRF BEAMLINE BL19U1 |
| Synchrotron site | SSRF |
| Beamline | BL19U1 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2015-12-31 |
| Detector | DECTRIS PILATUS 6M-F |
| Wavelength(s) | 0.9785 |
| Spacegroup name | P 65 2 2 |
| Unit cell lengths | 151.832, 151.832, 313.195 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 19.970 - 2.500 |
| R-factor | 0.221 |
| Rwork | 0.219 |
| R-free | 0.26200 |
| Structure solution method | SAD |
| RMSD bond length | 0.013 |
| RMSD bond angle | 1.135 |
| Data reduction software | XDS |
| Data scaling software | SCALA |
| Phasing software | PHENIX |
| Refinement software | PHENIX ((DEV_2247: ???)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 20.000 | 2.640 |
| High resolution limit [Å] | 2.500 | 2.500 |
| Number of reflections | 74200 | |
| <I/σ(I)> | 21 | |
| Completeness [%] | 99.8 | 100 |
| Redundancy | 40 | 41 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 6.75 | 283 | PEG4000, Li2SO4, 2-Proponal |
