5Y03

Galectin-13/Placental Protein 13 variant R53H crystal structure

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL18U1
Synchrotron site	SSRF
Beamline	BL18U1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2017-07-02
Detector	DECTRIS PILATUS3 6M
Wavelength(s)	0.98
Spacegroup name	C 2 2 2
Unit cell lengths	57.877, 92.314, 50.625
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	19.050 - 2.120
R-factor	0.1801
Rwork	0.175
R-free	0.22170
Refinement software	PHENIX (1.10.1_2155: ???)

Data quality characteristics

	Overall
Low resolution limit [Å]	19.052
High resolution limit [Å]	2.120
Number of reflections	7985
<I/σ(I)>	6.6
Completeness [%]	99.8
Redundancy	1.9

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		298	PEG