5XXF
Crystal structure of Poz1, Tpz1 and Rap1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL18U1 |
Synchrotron site | SSRF |
Beamline | BL18U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-06-13 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.97861 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 81.159, 85.741, 116.044 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 50.000 - 3.100 |
R-factor | 0.2526 |
Rwork | 0.250 |
R-free | 0.30230 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5xxe |
RMSD bond length | 0.007 |
RMSD bond angle | 1.118 |
Data scaling software | HKL-2000 |
Refinement software | REFMAC (5.8.0103) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 3.210 |
High resolution limit [Å] | 3.100 | 6.670 | 3.100 |
Rmerge | 0.101 | 0.056 | 0.732 |
Rmeas | 0.110 | 0.061 | 0.801 |
Rpim | 0.043 | 0.025 | 0.320 |
Number of reflections | 15449 | ||
<I/σ(I)> | 5.7 | ||
Completeness [%] | 100.0 | 99.8 | 100 |
Redundancy | 6.5 | 6.1 | 6.2 |
CC(1/2) | 0.996 | 0.819 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | EVAPORATION | 7 | 277 | 0.2 M Potassium nitrate, 20%(w/v) PEG3350 |