5XVR
EarP bound with dTDP-rhamnose (co-crystal)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL41XU |
Synchrotron site | SPring-8 |
Beamline | BL41XU |
Temperature [K] | 90 |
Detector technology | PIXEL |
Collection date | 2017-05-24 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 1 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 97.390, 195.190, 46.320 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 48.798 - 1.630 |
R-factor | 0.1652 |
Rwork | 0.164 |
R-free | 0.19990 |
Structure solution method | FOURIER SYNTHESIS |
RMSD bond length | 0.011 |
RMSD bond angle | 1.120 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHENIX |
Refinement software | PHENIX ((1.11.1_2575: ???)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 48.800 |
High resolution limit [Å] | 1.630 |
Number of reflections | 110150 |
<I/σ(I)> | 19.7 |
Completeness [%] | 99.1 |
Redundancy | 21.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 277 | 8% tacsimate pH 6.0, 12% PEG6000, 0.2M lithium sulfate, 10mM dTDP-rhamnose |