5XUL

Complex structure (RmMan134A-M6).

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL18U1
Synchrotron site	SSRF
Beamline	BL18U1
Temperature [K]	80
Detector technology	PIXEL
Collection date	2016-11-22
Detector	DECTRIS PILATUS3 6M
Wavelength(s)	0.977
Spacegroup name	P 21 21 21
Unit cell lengths	49.504, 59.145, 122.952
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	45.920 - 1.980
Rwork	0.160
R-free	0.20340
Structure solution method	MOLECULAR REPLACEMENT
Data reduction software	HKL-3000
Data scaling software	HKL-3000
Phasing software	PHENIX
Refinement software	PHENIX (dev-2474-000)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	45.920
High resolution limit [Å]	1.990	1.980
Rmerge	0.086	0.086
Number of reflections	23177
<I/σ(I)>	7.3
Completeness [%]	91.0	91
Redundancy	4.7	4.7

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		293	Tris-Hcl, tri-Sodium Citrate