5XRR
Crystal structure of FUS (54-59) SYSSYG
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U1 |
Synchrotron site | SSRF |
Beamline | BL17U1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2015-10-28 |
Detector | RAYONIX MX-225 |
Wavelength(s) | 0.9791 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 28.240, 30.270, 4.780 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 20.649 - 1.503 |
R-factor | 0.2098 |
Rwork | 0.204 |
R-free | 0.24070 |
RMSD bond length | 0.007 |
RMSD bond angle | 1.130 |
Data scaling software | XSCALE |
Refinement software | PHENIX (1.11.1_2575) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 20.649 | 20.649 | 1.600 |
High resolution limit [Å] | 1.500 | 10.000 | 1.500 |
Rmerge | 0.422 | 0.248 | 0.821 |
Rmeas | 0.453 | 0.270 | 0.881 |
Total number of observations | 9186 | ||
Number of reflections | 1197 | 6 | 194 |
<I/σ(I)> | 3.37 | 6.17 | 1.52 |
Completeness [%] | 94.3 | 100 | 75.8 |
Redundancy | 7.674 | 6.667 | 7.345 |
CC(1/2) | 0.972 | 0.998 | 0.711 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8 | 289 | 2.5 M NaCl, 0.1 M imidazole pH 8.0, 0.2 M zinc acetate |