5XRB
Crystal Structure of the human Hsp90-alpha N-domain bound to the hsp90 inhibitor FJ5
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U1 |
Synchrotron site | SSRF |
Beamline | BL17U1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2012-01-03 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.97915 |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 67.446, 90.701, 98.277 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 35.145 - 1.650 |
R-factor | 0.1877 |
Rwork | 0.187 |
R-free | 0.19770 |
RMSD bond length | 0.006 |
RMSD bond angle | 1.008 |
Data scaling software | HKL-2000 |
Refinement software | PHENIX (1.6.2_432) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 35.145 |
High resolution limit [Å] | 1.650 |
Number of reflections | 36575 |
<I/σ(I)> | 63.3 |
Completeness [%] | 100.0 |
Redundancy | 14.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP |