5XR7
Crystal structure of RabA1a (Q72K) in complex with GTP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PAL/PLS BEAMLINE 7A (6B, 6C1) |
Synchrotron site | PAL/PLS |
Beamline | 7A (6B, 6C1) |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2016-05-26 |
Detector | ADSC QUANTUM 270 |
Wavelength(s) | 1.0 |
Spacegroup name | P 1 |
Unit cell lengths | 37.570, 43.046, 67.609 |
Unit cell angles | 86.66, 74.07, 82.28 |
Refinement procedure
Resolution | 29.415 - 2.600 |
R-factor | 0.2229 |
Rwork | 0.216 |
R-free | 0.28550 |
RMSD bond length | 0.010 |
RMSD bond angle | 1.116 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX |
Refinement software | PHENIX (1.10.1_2155) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 2.600 |
Number of reflections | 12784 |
<I/σ(I)> | 26.9 |
Completeness [%] | 97.7 |
Redundancy | 3.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.5 | 293 | 0.1 M MES (pH5.5), 10 mM magnesium acetate, 2.2 M ammonium sulfate |