5XQW
Catalytic antibody 7B9
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | Cu FINE FOCUS |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2001-04-25 |
Detector | MAC Science DIP-2030 |
Wavelength(s) | 1.54 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 44.942, 61.904, 70.959 |
Unit cell angles | 90.00, 92.55, 90.00 |
Refinement procedure
Resolution | 14.970 - 2.200 |
R-factor | 0.19453 |
Rwork | 0.187 |
R-free | 0.26082 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1kb5 |
RMSD bond length | 0.014 |
RMSD bond angle | 1.700 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | AMoRE |
Refinement software | REFMAC (5.8.0135) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 2.300 |
High resolution limit [Å] | 2.200 | 2.200 |
Number of reflections | 19632 | |
<I/σ(I)> | 12.6 | 2.4 |
Completeness [%] | 98.8 | 95.5 |
Redundancy | 2.6 | 2.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8.5 | 293 | 100mM Tris HCl, 15%(w/v) PEG 1000, 5% 2-methyl-2,4-pentanediol |