5XQN
Crystal structure of Notched-fin eelpout type III antifreeze protein (NFE6, AFP), C2221 form.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE BL-6A |
Synchrotron site | Photon Factory |
Beamline | BL-6A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2006-11-03 |
Detector | ADSC QUANTUM 4r |
Wavelength(s) | 1.0 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 75.651, 108.248, 38.041 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 26.823 - 1.190 |
R-factor | 0.1353 |
Rwork | 0.134 |
R-free | 0.16180 |
Structure solution method | FOURIER SYNTHESIS |
RMSD bond length | 0.006 |
RMSD bond angle | 1.232 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.230 |
High resolution limit [Å] | 1.190 | 1.190 |
Number of reflections | 48626 | 4581 |
<I/σ(I)> | 88.4 | |
Completeness [%] | 96.3 | 92.2 |
Redundancy | 15 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 277 | 2.5 M Ammonium sulfate, 0.1 M Na-Citrate pH5.0 |