5XLX
Crystal structure of the C-terminal domain of CheR1 containing SAH
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL19U1 |
Synchrotron site | SSRF |
Beamline | BL19U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-03-08 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 0.9798 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 36.237, 78.392, 140.808 |
Unit cell angles | 90.00, 95.93, 90.00 |
Refinement procedure
Resolution | 40.111 - 1.969 |
R-factor | 0.1923 |
Rwork | 0.191 |
R-free | 0.22980 |
RMSD bond length | 0.002 |
RMSD bond angle | 0.652 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX (dev_2719) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 1.969 |
Number of reflections | 52220 |
<I/σ(I)> | 24.29 |
Completeness [%] | 98.8 |
Redundancy | 6.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.5 | 289 | 15%(w/v)PEG10,000 100mM Sodium citrate PH5.5 2%(V/V)Dioxane |