5XG7
Galectin-13/Placental Protein 13 crystal structure
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL18U1 |
Synchrotron site | SSRF |
Beamline | BL18U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-10-21 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.9 |
Spacegroup name | C 2 2 2 |
Unit cell lengths | 57.879, 92.104, 50.752 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 19.080 - 1.550 |
R-factor | 0.1622 |
Rwork | 0.159 |
R-free | 0.18730 |
Structure solution method | MOLECULAR REPLACEMENT |
Refinement software | REFMAC |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 19.080 |
High resolution limit [Å] | 1.550 |
Rmerge | 0.081 |
Number of reflections | 19963 |
<I/σ(I)> | 13.6 |
Completeness [%] | 95.6 |
Redundancy | 6.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | EVAPORATION | 298 | PEG |