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5XF1

Structure of the Full-length glucagon class B G protein-coupled receptor

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSPRING-8 BEAMLINE BL41XU
Synchrotron siteSPring-8
BeamlineBL41XU
Temperature [K]100
Detector technologyPIXEL
Collection date2016-07-20
DetectorDECTRIS PILATUS3 S 6M
Wavelength(s)1.000
Spacegroup nameP 1 21 1
Unit cell lengths71.460, 248.790, 93.330
Unit cell angles90.00, 90.16, 90.00
Refinement procedure
Resolution46.920 - 3.190
R-factor0.2066
Rwork0.205
R-free0.23148
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)4l6r
RMSD bond length0.011
RMSD bond angle1.397
Data reduction softwareXDS
Data scaling softwareXDS
Phasing softwarePHASER
Refinement softwareREFMAC (5.8.0103)
Data quality characteristics
 Overall
Low resolution limit [Å]50.000
High resolution limit [Å]3.190
Number of reflections49677
<I/σ(I)>3.1
Completeness [%]92.8
Redundancy2.8
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1LIPIDIC CUBIC PHASE293100mM HEPES, pH7.0, 200mM potassium phospphate monobasic, 20% PEG500DME, 10 mM gly-gly-glysine

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