5XAY
Crystal structure of full length tylp, a tetr regulator from streptomyces fradiae
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | OTHER |
Synchrotron site | Australian Synchrotron |
Beamline | MX2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-07-20 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.9686 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 101.329, 71.885, 160.066 |
Unit cell angles | 90.00, 102.54, 90.00 |
Refinement procedure
Resolution | 19.920 - 2.580 |
R-factor | 0.22813 |
Rwork | 0.227 |
R-free | 0.28386 |
Structure solution method | SAD |
RMSD bond length | 0.015 |
RMSD bond angle | 2.010 |
Data scaling software | Aimless |
Phasing software | Auto-Rickshaw |
Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 19.920 | 2.620 |
High resolution limit [Å] | 2.580 | 2.580 |
Rmerge | 0.542 | |
Number of reflections | 69940 | |
<I/σ(I)> | 2.9 | 2.9 |
Completeness [%] | 99.5 | |
Redundancy | 4.1 | 4.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 298 | 0.2M Ammonium citrate tribasic (pH 7.0), 20% w/v PEG 3350 |