5XAC
CLIR - LC3B
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE AR-NE3A |
Synchrotron site | Photon Factory |
Beamline | AR-NE3A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2016-02-18 |
Detector | ADSC QUANTUM 270 |
Wavelength(s) | 1.0 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 59.369, 73.641, 68.672 |
Unit cell angles | 90.00, 101.36, 90.00 |
Refinement procedure
Resolution | 35.338 - 1.701 |
R-factor | 0.2122 |
Rwork | 0.211 |
R-free | 0.24500 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3vtu |
RMSD bond length | 0.004 |
RMSD bond angle | 0.670 |
Data reduction software | DENZO |
Data scaling software | HKL-2000 |
Phasing software | PHENIX |
Refinement software | PHENIX ((1.11.1_2575)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 35.338 |
High resolution limit [Å] | 1.700 |
Number of reflections | 63531 |
<I/σ(I)> | 37.86 |
Completeness [%] | 99.7 |
Redundancy | 4.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 293 | PEG 3,350, 0.1M HEPES pH 7.5, 200mM NaCl. |