5X9U
Crystal structure of group III chaperonin in the open state
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE BL-1A |
Synchrotron site | Photon Factory |
Beamline | BL-1A |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-05-23 |
Detector | DECTRIS PILATUS 2M |
Wavelength(s) | 1.10000 |
Spacegroup name | P 4 21 2 |
Unit cell lengths | 209.780, 209.780, 169.813 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 4.000 |
Number of reflections | 32570 |
<I/σ(I)> | 8.4 |
Completeness [%] | 99.7 |
Redundancy | 20.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | MICROBATCH | 295 | 3 mM ADP, 200 mM NH4Cl, 10mM MgCl2, 50mM HEPES sodium (pH 7.0), 5% w/v Polyethylene glycol PEG 8000, 3% 1,8-Diaminooctane |