Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE BM14 |
| Synchrotron site | ESRF |
| Beamline | BM14 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2005-06-05 |
| Detector | MARRESEARCH |
| Wavelength(s) | 0.88560 |
| Spacegroup name | P 43 21 2 |
| Unit cell lengths | 60.570, 60.570, 241.050 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 19.581 - 3.000 |
| R-factor | 0.248 |
| Rwork | 0.246 |
| R-free | 0.29120 |
| Structure solution method | SAD |
| RMSD bond length | 0.006 |
| RMSD bond angle | 1.056 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | RESOLVE |
| Refinement software | PHENIX (1.8.4_1496) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 19.581 | 3.340 |
| High resolution limit [Å] | 3.000 | 3.000 |
| Rmerge | 0.080 | 0.480 |
| Number of reflections | 9599 | |
| <I/σ(I)> | 35.14 | 2.4 |
| Completeness [%] | 98.7 | 97.6 |
| Redundancy | 13.7 | 12.3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 293 | 0.1M HEPES, 12% PEG 10K, 0.1M AMMONIUM SULFATE, 0.5% BETA-OCTYL GLUCOSIDE |
