5X6E
Crystal structure of PrfA-DNA binary complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-E |
Synchrotron site | APS |
Beamline | 24-ID-E |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2016-04-05 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.9791 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 65.017, 96.590, 370.528 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 93.466 - 2.990 |
R-factor | 0.2515 |
Rwork | 0.249 |
R-free | 0.29970 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.007 |
RMSD bond angle | 1.278 |
Phasing software | PHASER |
Refinement software | PHENIX (1.8.4_1496) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 96.620 |
High resolution limit [Å] | 2.990 |
Number of reflections | 46496 |
<I/σ(I)> | 8.7 |
Completeness [%] | 88.8 |
Redundancy | 4.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.1M Tris, 27% PEG3350, 0.2M Li2SO4, pH 8.5 |