5X3O
Crystal structure of p-DiUb-S65-COOH
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-12-26 |
Detector | DECTRIS PILATUS 200K |
Wavelength(s) | 1.54 |
Spacegroup name | P 1 2 1 |
Unit cell lengths | 40.608, 33.764, 44.686 |
Unit cell angles | 90.00, 103.49, 90.00 |
Refinement procedure
Resolution | 43.453 - 2.194 |
R-factor | 0.2445 |
Rwork | 0.240 |
R-free | 0.31530 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.008 |
RMSD bond angle | 1.089 |
Data reduction software | HKL-3000 |
Refinement software | PHENIX ((1.11.1_2575: ???)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 43.453 |
High resolution limit [Å] | 2.194 |
Number of reflections | 6127 |
<I/σ(I)> | 2.53 |
Completeness [%] | 98.5 |
Redundancy | 6.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 289 | 0.2M Ammonium phosphate monobasic, 20%(w/v) Polyethylene glycol 3350 |