5X3N

Crystal structure of DiUb-K6

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	RIGAKU MICROMAX-007
Temperature [K]	100
Detector technology	PIXEL
Collection date	2017-01-09
Detector	DECTRIS PILATUS 200K
Wavelength(s)	1.54
Spacegroup name	P -1
Unit cell lengths	26.048, 26.278, 46.193
Unit cell angles	102.05, 94.14, 99.63

Refinement procedure

Resolution	44.896 - 1.649
R-factor	0.219
Rwork	0.216
R-free	0.27590
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.006
RMSD bond angle	0.832
Data reduction software	HKL-3000
Refinement software	PHENIX ((1.10.1_2155: ???))

Data quality characteristics

	Overall
Low resolution limit [Å]	44.896
High resolution limit [Å]	1.649
Number of reflections	11102
<I/σ(I)>	2.35
Completeness [%]	78.5
Redundancy	3.3

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		289	0.2M Magnesium formate dihydrate, 20%(w/v) Polyethylene glycol 3350