5X3C

Solution structure of the Family 1 carbohydrate-binding module Y5A mutant with mannosylated Ser3

Spectrometer

Experimental method: SOLUTION NMR

Spectrometer ID	Spectrometer maker	Spectrometer model	Spectrometer type	Spectrometer field strength
1	Bruker	AVANCE III		600

Experiment

experiment id	conditions id	solution id	Experiment type
1	1	1	2D 1H-1H TOCSY
10	1	2	2D 1H-13C HSQC
11	1	2	2D 1H-13C HSQC-TOCSY
12	1	2	2D 1H-13C H2BC
2	1	1	2D DQF-COSY
3	1	1	2D 1H-1H NOESY
4	1	1	2D 1H-13C HSQC
5	1	1	2D 1H-13C HSQC-TOCSY
6	1	1	2D 1H-15N HSQC
7	1	2	2D 1H-1H TOCSY
8	1	2	2D DQF-COSY
9	1	2	2D 1H-1H NOESY

NMR Sample

conditions id	NMR sample pH	NMR sample pressure	NMR sample temperature
1	5	1	298

Conformers

Conformers Calculated Total Number	100
Conformers Submitted Total Number	20