5WZI
Structure of APUM23-GGAGUUGACGG
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2016-09-19 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.97916 |
Spacegroup name | P 65 |
Unit cell lengths | 190.497, 190.497, 45.727 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 39.993 - 2.750 |
R-factor | 0.1914 |
Rwork | 0.189 |
R-free | 0.24190 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5wzg |
RMSD bond length | 0.008 |
RMSD bond angle | 0.932 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX (1.11.1_2575) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 40.000 | 40.000 | 2.800 |
High resolution limit [Å] | 2.750 | 7.450 | 2.750 |
Rmerge | 0.143 | 0.067 | 0.777 |
Rmeas | 0.150 | 0.070 | 0.812 |
Rpim | 0.043 | 0.020 | 0.234 |
Number of reflections | 25175 | ||
<I/σ(I)> | 6.5 | ||
Completeness [%] | 100.0 | 99.9 | 100 |
Redundancy | 11.9 | 11.3 | 11.8 |
CC(1/2) | 0.997 | 0.914 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7 | 293 | 0.15 M DL-Malic acid (pH 7.0), 20% w/v Polyethylene glycol 3350 |