5WYL
Crystal structure of Chaetomium thermophilum Utp10 N-terminal domain in complex with Utp17 C-terminal helices
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2015-01-25 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.9793 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 98.309, 98.309, 235.653 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 39.010 - 2.638 |
R-factor | 0.215 |
Rwork | 0.212 |
R-free | 0.26670 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5wy4 |
RMSD bond length | 0.009 |
RMSD bond angle | 1.029 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHENIX |
Refinement software | PHENIX ((1.11rc1_2513: ???)) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 49.154 | 49.154 | 2.800 |
High resolution limit [Å] | 2.640 | 7.820 | 2.640 |
Rmerge | 0.077 | 0.078 | 0.185 |
Rmeas | 0.078 | 0.080 | 0.188 |
Total number of observations | 943385 | ||
Number of reflections | 34951 | 1508 | 5518 |
<I/σ(I)> | 35.46 | 50.14 | 15.87 |
Completeness [%] | 100.0 | 99.3 | 99.9 |
Redundancy | 26.992 | ||
CC(1/2) | 0.999 | 0.997 | 0.997 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 293 | 0.1 M Hepes-Na, 20% w/v PEG 8000 |