5WY4
Crystal structure of Chaetomium thermophilum Utp10 N-terminal domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2013-12-28 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.9792 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 81.888, 70.458, 93.728 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 19.908 - 2.499 |
R-factor | 0.2263 |
Rwork | 0.222 |
R-free | 0.26380 |
Structure solution method | SAD |
RMSD bond length | 0.009 |
RMSD bond angle | 0.979 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | PHENIX |
Refinement software | PHENIX ((1.11rc1_2513: ???)) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 2.540 |
High resolution limit [Å] | 2.500 | 6.781 | 2.500 |
Rmerge | 0.103 | 0.062 | 0.461 |
Total number of observations | 168375 | ||
Number of reflections | 35781 | ||
<I/σ(I)> | 15.9 | ||
Completeness [%] | 98.6 | 85 | 100 |
Redundancy | 4.7 | 3.6 | 3.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.6 | 293 | 0.1 M sodium citrate, 1.0 M ammonium dihydrogen phosphate |