5WXJ
Apo EarP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL32XU |
Synchrotron site | SPring-8 |
Beamline | BL32XU |
Temperature [K] | 90 |
Detector technology | CCD |
Collection date | 2015-09-30 |
Detector | RAYONIX MX225-HS |
Wavelength(s) | 1 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 97.622, 195.774, 46.396 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 47.361 - 1.850 |
R-factor | 0.1592 |
Rwork | 0.158 |
R-free | 0.19770 |
Structure solution method | SAD |
RMSD bond length | 0.017 |
RMSD bond angle | 1.363 |
Data scaling software | Aimless |
Phasing software | SHELXCD |
Refinement software | PHENIX ((1.11.1_2575: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.940 | 1.890 |
High resolution limit [Å] | 1.850 | 1.850 |
Number of reflections | 77019 | |
<I/σ(I)> | 11.5 | 2 |
Completeness [%] | 100.0 | 99.8 |
Redundancy | 7.4 | 7.1 |
CC(1/2) | 0.704 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 277 | 0.1 M Hepes-NaOH buffer (pH 6.8-7.5), 20% PEG3350, and 0.2 M ammonium sulfate |