Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE AR-NW12A |
Synchrotron site | Photon Factory |
Beamline | AR-NW12A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2003-11-07 |
Detector | ADSC QUANTUM 210 |
Wavelength(s) | 1.0000 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 170.100, 233.700, 124.400 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 41.245 - 2.600 |
R-factor | 0.1924 |
Rwork | 0.190 |
R-free | 0.23390 |
RMSD bond length | 0.014 |
RMSD bond angle | 1.245 |
Data scaling software | HKL-2000 |
Phasing software | MOLREP |
Refinement software | PHENIX ((1.10.1_2155: ???)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 41.245 |
High resolution limit [Å] | 2.600 |
Number of reflections | 75787 |
<I/σ(I)> | 6.9 |
Completeness [%] | 99.4 |
Redundancy | 3.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7 | 278 | PEG 8000, posodium chloride, magnesium chloride, Tris-HCl |