5WUD
Structural basis for conductance through TRIC cation channels
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-E |
Synchrotron site | APS |
Beamline | 24-ID-E |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-08-26 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 0.8153 |
Spacegroup name | P 63 |
Unit cell lengths | 64.613, 64.613, 80.955 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 46.031 - 1.900 |
R-factor | 0.1886 |
Rwork | 0.187 |
R-free | 0.21960 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5wuc |
Data reduction software | XDS |
Data scaling software | Aimless (0.5.28) |
Phasing software | PHASER |
Refinement software | PHENIX (dev_2481) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 46.031 | 46.030 | 1.840 |
High resolution limit [Å] | 1.800 | 9.000 | 1.800 |
Rmerge | 0.025 | 0.033 | 0.492 |
Number of reflections | 17832 | ||
<I/σ(I)> | 14.5 | ||
Completeness [%] | 100.0 | 99.4 | 99.4 |
Redundancy | 20.3 | 21 | 20.4 |
CC(1/2) | 0.999 | 1.000 | 0.318 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | LIPIDIC CUBIC PHASE | 7 | 291 | PEG 200 38%, RbCl 100mM, MgCl2 100mM, HEPES pH 7.0 100mM |