5WU6
Crystal structure of apo human Tut1, form IV
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE BL-17A |
Synchrotron site | Photon Factory |
Beamline | BL-17A |
Temperature [K] | 95 |
Detector technology | PIXEL |
Collection date | 2015-12-07 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 0.98 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 142.530, 142.530, 282.690 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 19.993 - 3.209 |
R-factor | 0.2043 |
Rwork | 0.202 |
R-free | 0.24180 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5wu1 |
RMSD bond length | 0.003 |
RMSD bond angle | 0.770 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX (1.8.4_1496) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 3.290 | |
High resolution limit [Å] | 3.200 | 14.350 | 3.210 |
Rmerge | 0.375 | 0.050 | 2.345 |
Number of reflections | 48397 | ||
<I/σ(I)> | 14.32 | 57.42 | 1.88 |
Completeness [%] | 99.9 | 96.7 | 98.9 |
Redundancy | 26.4 | ||
CC(1/2) | 0.995 | 1.000 | 0.677 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 277 | Tris pH 7.0, PEG3350, MgCl2. |