5WSH
Structure of HLA-A2 P130
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRF BEAMLINE BL17U |
| Synchrotron site | SSRF |
| Beamline | BL17U |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2011-03-06 |
| Detector | SDMS |
| Wavelength(s) | 1.0 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 112.159, 78.675, 60.295 |
| Unit cell angles | 90.00, 96.93, 90.00 |
Refinement procedure
| Resolution | 28.003 - 2.000 |
| R-factor | 0.1632 |
| Rwork | 0.162 |
| R-free | 0.19620 |
| RMSD bond length | 0.005 |
| RMSD bond angle | 0.874 |
| Data reduction software | CNS |
| Data scaling software | CNS |
| Phasing software | CNS |
| Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 50.000 |
| High resolution limit [Å] | 2.000 |
| <I/σ(I)> | 22.61 |
| Completeness [%] | 99.7 |
| Redundancy | 5.3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 291 | 0.1mol/L bis-tris(pH6.5), 20%(wt/vol) polyethylene glycol 3350 |
