5WR9
Crystal structure of hen egg-white lysozyme
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | FREE ELECTRON LASER |
| Source details | SACLA BEAMLINE BL3 |
| Synchrotron site | SACLA |
| Beamline | BL3 |
| Temperature [K] | 299 |
| Detector technology | CCD |
| Collection date | 2015-10-06 |
| Detector | MPCCD |
| Wavelength(s) | 1.24 |
| Spacegroup name | P 43 21 2 |
| Unit cell lengths | 80.000, 80.000, 38.400 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 30.000 - 1.800 |
| R-factor | 0.1754 |
| Rwork | 0.175 |
| R-free | 0.18380 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.059 |
| Data scaling software | CrystFEL |
| Refinement software | PHENIX (1.8.4_1496) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 30.000 |
| High resolution limit [Å] | 1.800 |
| Number of reflections | 12068 |
| <I/σ(I)> | 10.2 |
| Completeness [%] | 100.0 |
| Redundancy | 399 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | BATCH MODE | 285 | sodium chloride, PEG 6000, pH 3.0 |
