5WPY
Solution Structure of KstB-PCP loaded with nicotinic acid in kosinostatin biosynthesis
Spectrometer
Experimental method: SOLUTION NMR
Spectrometer ID | Spectrometer maker | Spectrometer model | Spectrometer type | Spectrometer field strength |
1 | Varian | INOVA | 600 |
Experiment
experiment id | conditions id | solution id | Experiment type |
1 | 1 | 1 | 2D 1H-15N HSQC |
10 | 1 | 1 | 3D HCCH-TOCSY |
11 | 1 | 1 | 3D 1H-15N TOCSY |
2 | 1 | 1 | 2D 1H-13C HSQC |
3 | 1 | 1 | 3D CBCA(CO)NH |
4 | 1 | 1 | 3D HNCO |
5 | 1 | 1 | 3D HNCA |
6 | 1 | 1 | 3D 1H-13C NOESY |
7 | 1 | 1 | 3D 1H-15N NOESY |
8 | 1 | 1 | 3D HN(CO)CA |
9 | 1 | 1 | 3D HNCACB |
NMR Sample
conditions id | NMR sample pH | NMR sample pressure | NMR sample temperature |
1 | 7 | 1 | 293 |
Conformers
Conformers Calculated Total Number | 100 |
Conformers Submitted Total Number | 20 |