5WPI
The virulence-associated protein HsvA from the fire blight pathogen Erwinia amylovora is a polyamine amidinotransferase
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU FR-E SUPERBRIGHT |
Temperature [K] | 80 |
Detector technology | IMAGE PLATE |
Collection date | 2012-02-02 |
Detector | RIGAKU |
Wavelength(s) | 1.54 |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 127.543, 127.543, 92.229 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 38.030 - 2.300 |
R-factor | 0.173 |
Rwork | 0.170 |
R-free | 0.22600 |
RMSD bond length | 0.008 |
RMSD bond angle | 0.879 |
Data reduction software | d*TREK |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX ((1.11.1_2575: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 38.030 | 2.380 |
High resolution limit [Å] | 2.300 | 2.300 |
Rmerge | 0.117 | 0.517 |
Number of reflections | 38767 | |
<I/σ(I)> | 7.9 | 2.5 |
Completeness [%] | 100.0 | 100 |
Redundancy | 5.93 | 5.88 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 293 | 0.2 M MgCl2, 0.1 M HEPES pH 7.5, and 30% (w/v) PEG 400 |