Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 21-ID-D |
Synchrotron site | APS |
Beamline | 21-ID-D |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2013-08-24 |
Detector | MARMOSAIC 300 mm CCD |
Wavelength(s) | 0.97933 |
Spacegroup name | P 41 2 2 |
Unit cell lengths | 43.090, 43.090, 258.669 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 30.469 - 1.870 |
R-factor | 0.2107 |
Rwork | 0.207 |
R-free | 0.24780 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5INA |
RMSD bond length | 0.014 |
RMSD bond angle | 1.244 |
Data reduction software | iMOSFLM |
Data scaling software | Aimless |
Phasing software | PHENIX |
Refinement software | PHENIX ((1.12_2829: ???)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 30.480 |
High resolution limit [Å] | 1.870 |
Number of reflections | 21505 |
<I/σ(I)> | 13.8 |
Completeness [%] | 100.0 |
Redundancy | 9.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 8 | 293 | PEG 3000, imidazole, zinc acetate |