Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 21-ID-D |
| Synchrotron site | APS |
| Beamline | 21-ID-D |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2013-08-19 |
| Detector | MARMOSAIC 300 mm CCD |
| Wavelength(s) | 1.28367 |
| Spacegroup name | P 41 2 2 |
| Unit cell lengths | 42.900, 42.900, 260.200 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 27.490 - 1.790 |
| R-factor | 0.22 |
| Rwork | 0.218 |
| R-free | 0.23800 |
| Structure solution method | SAD |
| RMSD bond length | 0.013 |
| RMSD bond angle | 1.244 |
| Data reduction software | iMOSFLM |
| Data scaling software | Aimless |
| Phasing software | PHENIX |
| Refinement software | PHENIX (1.10.1_2155) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 30.500 |
| High resolution limit [Å] | 1.790 |
| Number of reflections | 41701 |
| <I/σ(I)> | 7 |
| Completeness [%] | 94.0 |
| Redundancy | 4.3 |
| CC(1/2) | 0.998 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 8 | 293 | PEG 3000, imidazole, zinc acetate |
