5WM7
Crystal Structure of CahJ in Complex with AMP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 23-ID-D |
Synchrotron site | APS |
Beamline | 23-ID-D |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-06-07 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 1.03320 |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 121.916, 121.916, 87.996 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 45.270 - 1.777 |
R-factor | 0.1452 |
Rwork | 0.136 |
R-free | 0.17370 |
Structure solution method | FOURIER SYNTHESIS |
Starting model (for MR) | 5wm2 |
RMSD bond length | 0.006 |
RMSD bond angle | 0.851 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHENIX |
Refinement software | PHENIX (1.11.1_2575) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 45.270 | 45.270 | 1.880 |
High resolution limit [Å] | 1.777 | 5.300 | 1.777 |
Rmerge | 0.098 | 0.038 | 0.777 |
Rmeas | 0.110 | 0.043 | 0.883 |
Number of reflections | 70015 | 2694 | 11102 |
<I/σ(I)> | 11.37 | 34.01 | 1.76 |
Completeness [%] | 96.1 | 92.3 | 95.1 |
Redundancy | 4.064 | 4.006 | 4.02 |
CC(1/2) | 0.996 | 0.997 | 0.458 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | 293 | 100 mM Sodium Cacodylate pH 6.5, 1.7 M Sodium Acetate |