5WJO
Crystal structure of the unliganded PG90 TCR
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
Synchrotron site | Australian Synchrotron |
Beamline | MX2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2015-07-27 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.954 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 41.150, 128.080, 169.680 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 39.180 | 2.600 |
High resolution limit [Å] | 2.500 | 2.500 |
Rpim | 0.013 | 0.057 |
Number of reflections | 32046 | 3558 |
<I/σ(I)> | 6.8 | 2.1 |
Completeness [%] | 100.0 | 100 |
Redundancy | 6.9 | 6.6 |
CC(1/2) | 0.982 | 0.607 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 22% PEG 3350, 0.2M Magnesium Formate |