5WHV
Crystal structure of ArtB
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-08-21 |
Detector | RIGAKU SATURN 944 |
Wavelength(s) | 1.5418 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 140.872, 94.231, 125.230 |
Unit cell angles | 90.00, 103.62, 90.00 |
Refinement procedure
Resolution | 31.124 - 2.303 |
R-factor | 0.169 |
Rwork | 0.167 |
R-free | 0.21300 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4rhr |
RMSD bond length | 0.008 |
RMSD bond angle | 1.189 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX (1.8.1_1168) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 2.300 |
Number of reflections | 68092 |
<I/σ(I)> | 17.42 |
Completeness [%] | 96.6 |
Redundancy | 3.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 297 | peg 200, calcium chloride |