5WFU
Structural basis for the interaction of 14-3-3beta with Tricarboxylic Acid Cycle intermediate Malate
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 19-ID |
Synchrotron site | APS |
Beamline | 19-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2017-02-16 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.97929 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 256.392, 85.604, 56.066 |
Unit cell angles | 90.00, 101.73, 90.00 |
Refinement procedure
Resolution | 46.960 - 1.970 |
R-factor | 0.19157 |
Rwork | 0.190 |
R-free | 0.22435 |
RMSD bond length | 0.019 |
RMSD bond angle | 1.874 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | PHENIX |
Refinement software | REFMAC (5.7.0032) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 1.970 |
Number of reflections | 83288 |
<I/σ(I)> | 21.9 |
Completeness [%] | 99.2 |
Redundancy | 5.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | EVAPORATION | 7 | 291 | 2.1M DL-Malic Acid pH7.0 |