5WF9
Tepsin tENTH domain 1-153
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 21-ID-F |
Synchrotron site | APS |
Beamline | 21-ID-F |
Temperature [K] | 80 |
Detector technology | CCD |
Collection date | 2014-10-27 |
Detector | RAYONIX MX-300 |
Wavelength(s) | 0.979 |
Spacegroup name | P 4 21 2 |
Unit cell lengths | 90.180, 90.180, 42.770 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 45.090 - 1.800 |
R-factor | 0.1907 |
Rwork | 0.189 |
R-free | 0.21990 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5wfb |
RMSD bond length | 0.004 |
RMSD bond angle | 0.645 |
Data reduction software | xia2 |
Data scaling software | xia2 |
Phasing software | PHASER |
Refinement software | PHENIX ((1.11.1_2575: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 63.800 | 1.830 |
High resolution limit [Å] | 1.800 | 1.800 |
Rmerge | 0.103 | 1.905 |
Rpim | 0.020 | 0.462 |
Number of reflections | 16739 | |
<I/σ(I)> | 24.9 | 1.5 |
Completeness [%] | 98.9 | 91.6 |
Redundancy | 26.8 | 17.4 |
CC(1/2) | 1.000 | 0.534 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293.15 | 150mM MES monohydrate pH 6.0, 15% (w/v) PEG6000. |